Effect of TiO2nanoparticles on tensile strength of dental acrylic resins

Abstract

Background and aims. Adding further fillers to dental resins may enhance their physical characteristics. The aim of this study was to evaluate the tensile strength of heat-curing acrylic resin reinforced by TiO2nanoparticles added into the resin matrix.Materials and methods. Commercially available TiO2nanoparticles were obtained and characterized using X-ray diffrac-tion (XRD) and scanning electron microscopy (SEM) to determine their crystalline structure, particle size and morphology. TiO2-acrylic resin nanocomposite was prepared by mixing 0.5, 1 and 2 (wt%) of surface modified TiO2nanoparticles in an amalgamator providing three groups of samples. Before curing, the obtained paste was packed into steel molds. After cur-ing, the specimens were removed from the molds. The tensile strength test samples were prepared according to ISO 1567.Results. Two crystalline phases were found in TiO2nanoparticles including: (i) anatase as the major one, and (ii) rutile. The average particle size calculated according to the Scherrer equation was 20.4 nm, showing a normal size distribution. Ac-cording to SEM images, the nanocomposite with 1wt% TiO2nanoparticles had a better distribution compared to other groups. In addition, the group by 1wt% TiO2exhibited highertensile strength with a significant difference compared to other groups. ANOVA showed significant differences between the contents of TiO2particles in acrylic resin (F = 22.19; P < 0.001).Conclusion. A considerable increase in tensile strength was observed with titania NPs reinforcement agents in 1wt% by weight. Further increase of TiO2nanoparticles decreased the tensile strength. © 2014 The Authors; Tabriz University of Medical Sciences.